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Selective palladium-catalyzed amination of the heterocyclic core of variolins

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Authors
Baeza García, AlejandroUniversity of Alcalá Author; Burgos García, CarolinaUniversity of Alcalá Author; Álvarez-Builla Gómez, JulioUniversity of Alcalá Author; Vaquero López, Juan J.
Identifiers
Permanent link (URI): http://hdl.handle.net/10017/2652
DOI: 10.1016/j.tetlet.2007.02.011
ISSN: 0040-4039
Publisher
Elsevier
Date
2007
Affiliation
Universidad de Alcalá. Departamento de Química Orgánica
Funders
We acknowledge financial support from the Spanish Ministerio de Educación y Ciencia (project CTQ2005/011060), Comunidad de Madrid (CAM) and Universidad de Alcalá (UAH) (project CAM/UAH-2005/044) and a grant (A.B.) from the Ministerio de Educación y Ciencia.
Bibliographic citation
Tetrahedron Letters, 2007, v. 48, n. 14, p. 2597-2601
Keywords
Pyrido[3 ',3 ': 4,5]pyrrolo[1,2-c]pyrimidine
N-tosylmethyl dichloroformimide
Amination
Palladium-catalyzed
Variolins
Sponge kirkpatrickia-varialosa
Tosylmethyl isocyanide
Alkaloids
Deoxyvariolin-B
Azolopyrimidines
Meridianins
Derivatives
Chlorides
Oxazoles
Bromides
Chemistry, Organic
Project
CTQ2005/011060 (Ministerio de Educación y Ciencia)
CAM/UAH-2005/044 (Comunidad de Madrid)
Document type
info:eu-repo/semantics/article
Version
info:eu-repo/semantics/publishedVersion
Publisher's version
http://dx.doi.org/10.1016/j.tetlet.2007.02.011
Rights
(c) Elsevier, 2007
Access rights
info:eu-repo/semantics/openAccess
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Abstract
A new and selective palladium-catalyzed amination of the pyrido[3′,3′:4,5]pyrrolo[1,2-c]pyrimidine nucleus, the heterocyclic core of the variolin alkaloids, is described. The method allows the introduction of amino and aryl- and alkylamino substituents on the C9 position in advanced precursors of variolin B and deoxyvariolin.
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